Cyclohexaneacetic acid → HCID 9970109, compound

HRID 2396278Notes

Reaction equation

HRID 2396278 reaction equation
CC([C:4]1[CH:9]=[CH:8][CH:7]=[C:6](C(C)C)[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.C(C1C=CC=C(C(C)C)C=1CC(O)=O)(C)C.C1(CC(O)=O)CCCCC1>>[CH:5]1([CH2:13][C:14]([C:16]2[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=2)=[O:15])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:4]1

Participants

4

Reactant 3

HCID 21363Cyclohexaneacetic acidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 9970109HCID 9970109, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with cyclohexylacetic acid; 1H NMR (CDCl3): δ 8.35 (s, 1H), 7.1-7.3 (m, 3H), 3.3-3.45 (m, 2H), 2.35 (d, 2H), 1.55-1.95 (m, 8H), 1.22 (d, 12H) , 0.9-1.1 (m, 2H), ppm.

Sources & evidence

ORD record
ord-cd81eb48c6fe4ee29ea9b94cdc2c4ca8
Source dataset
uspto-grants-1996_02
Patent number
US05491172

Reaction notes

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