2-Phenylbutyryl chloride → Sulfamic acid(1-oxo-2-phenylbutyl)-2,6-bis(1-methylethyl)phenyl ester

HRID 2396282Notes

Reaction equation

HRID 2396282 reaction equation
[CH3:1][CH:2]([C:4]1C=CC=[C:6]([CH:10](C)C)[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.[CH:33](C1C=CC=C(C(C)C)C=1CC(Cl)=O)(C)[CH3:34].C1(C(CC)C(Cl)=O)C=CC=CC=1>>[O:15]=[C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)[CH:13]([C:5]1[CH:4]=[CH:2][CH:1]=[CH:10][CH:6]=1)[CH2:33][CH3:34]

Participants

4

Reactant 3

HCID 981732-Phenylbutyryl chlorideHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 193627822,6-Diisopropylphenylacetyl chloride

Product 1

HCID 18988692Sulfamic acid(1-oxo-2-phenylbutyl)-2,6-bis(1-methylethyl)phenyl ester

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetyl chloride was replaced with 2-phenylbutyryl chloride, mp 142°-145° C.

Sources & evidence

ORD record
ord-ba0c77e5cb61499f87b64cea22d0f865
Source dataset
uspto-grants-1996_02
Patent number
US05491172

Reaction notes

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