Bis(4-chlorophenyl)acetic acid → HCID 19046543, compound

HRID 2396285Notes

Reaction equation

HRID 2396285 reaction equation
CC(C1C=CC=C(C(C)C)C=1CC([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=O)C.C(C1C=CC=C(C(C)C)C=1CC(O)=O)(C)C.[Cl:49][C:50]1[CH:55]=[CH:54][C:53]([CH:56]([C:60]2[CH:65]=[CH:64][C:63]([Cl:66])=[CH:62][CH:61]=2)[C:57](O)=[O:58])=[CH:52][CH:51]=1>>[Cl:49][C:50]1[CH:51]=[CH:52][C:53]([CH:56]([C:60]2[CH:61]=[CH:62][C:63]([Cl:66])=[CH:64][CH:65]=2)[C:57]([C:16]2[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=2)=[O:58])=[CH:54][CH:55]=1

Participants

4

Reactant 3

HCID 6730Bis(4-chlorophenyl)acetic acidHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 19046543HCID 19046543, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with bis(4-chlorophenyl)acetic acid, mp 175°-176° C.

Sources & evidence

ORD record
ord-8abfcfa6312c4b28bc3f1c57871fa69c
Source dataset
uspto-grants-1996_02
Patent number
US05491172

Reaction notes

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