9-Carboxyfluorene → HCID 10225810, compound

HRID 2396287Notes

Reaction equation

HRID 2396287 reaction equation
CC([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[CH2:13][C:14]([C:16]1[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:29])(=[O:28])[NH2:27])[C:19]([CH:22]([CH3:24])[CH3:23])=[CH:20][CH:21]=1)=[O:15])C.[CH:33](C1C=CC=C(C(C)C)C=1CC(O)=O)([CH3:35])[CH3:34].C1C2C(C(O)=O)C3C(=CC=CC=3)C=2C=CC=1>>[CH:4]1[C:5]2[CH:13]([C:14]([C:16]3[C:17]([CH:30]([CH3:32])[CH3:31])=[C:18]([O:25][S:26](=[O:28])(=[O:29])[NH2:27])[C:19]([CH:22]([CH3:23])[CH3:24])=[CH:20][CH:21]=3)=[O:15])[C:11]3[C:10](=[CH:12][CH:34]=[CH:33][CH:35]=3)[C:6]=2[CH:7]=[CH:8][CH:9]=1

Participants

4

Reactant 3

HCID 748099-CarboxyfluoreneHCID 10226443Sulfamic acid[[2,6-bis(1-methylethyl)phenyl]-acetyl]-2,6-bis(1-methylethyl)phenyl esterHCID 152779902-(2,6-Diisopropylphenyl)acetic acid

Product 1

HCID 10225810HCID 10225810, compound

Procedure

This compound was prepared in the same manner as for the title compound of Example 1, except that 2,6-diisopropylphenylacetic acid was replaced with 9-fluorenecarboxylic acid, mp 146°-147° C.

Sources & evidence

ORD record
ord-703ae5a3dac649b89f705ddd0b4ac06a
Source dataset
uspto-grants-1996_02
Patent number
US05491172

Reaction notes

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