HCID 10366410, compound → HCID 10341972, compound

HRID 2396512Notes

Reaction equation

HRID 2396512 reaction equation
[CH3:1][CH:2]([CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13]1[CH:18]=[C:17]([C:19]2[CH:24]=[CH:23][C:22]([N+:25]([O-])=O)=[CH:21][CH:20]=2)[CH:16]=[C:15]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[N:14]=1)[C:3]([O:5][CH2:6][CH3:7])=[O:4]>C(O)C>[CH3:1][CH:2]([CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13]1[CH:18]=[C:17]([C:19]2[CH:24]=[CH:23][C:22]([NH2:25])=[CH:21][CH:20]=2)[CH:16]=[C:15]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[N:14]=1)[C:3]([O:5][CH2:6][CH3:7])=[O:4]

Participants

3

Reactant 1

HCID 10366410HCID 10366410, compound

Product 1

HCID 10341972HCID 10341972, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The procedure in Example 12 is followed but using ethyl 2-methyl-6-{[4-(4-nitrophenyl)-6-phenyl-2-pyridyl]oxy}hexanoate (2.5 g), stannous chloride (5.3 g) and ethanol (100 cc). The residue, after extraction and concentration of the organic phases to dryness, is used as it is in the next stage. (yellow oil)

Workup

  1. extractionThe residue, after extraction and concentration of the organic phases to dryness

Sources & evidence

ORD record
ord-69a31712b7024ee5b3ec491c55ad4bac
Source dataset
uspto-grants-1996_02
Patent number
US05492915

Reaction notes

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