HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18987245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 18987360 | HCID 18987360 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18987245 | HCID 18987245 | 54% |
Reaction Steps
By using a similar procedure to that described in example 1 but with 1 g of ethyl 6-(3,5-diphenyl-phenoxy)hexanoate, 0.22 g of potassium hydroxide in pellets, 5 cc of water and 5 cc of ethanol as the starting material (2 hours; reflux), and after recrystallization in a mixture of 10 cc of n-hexane and 2 cc of ethyl acetate, 0.5 g (54%) of 6-(3,5-diphenyl-phenoxy)hexanoic acid was obtained as a white solid. (m.p.=104° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05492915 |
| Source dataset | uspto-grants-1996_02 |
| ORD ID | ord-4688274340a147e997f39cbe67fd8c61 |
| Source note | uspto-grants-1996_02 |