Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Dibutylamine | HCID 8148 | — |
| Reactant | Methallyl alcohol | HCID 10557 | — |
| Reactant | 4-Hydroxy-2,3,6-trimethylphenyl acetate | HCID 119024 | — |
| Product | HCID 18986673 | HCID 18986673 | — |
Reaction Steps
A pressure-proof reaction vessel equipped with a stirrer was charged with 17.5 g (0.09 mole) of 4-acetoxy-2,3,5-trimethylphenol, 32.5 g (0.45 mole) of 2-methyl-2-propen-1-ol, 3.7 g (0.099 mole) of 80% paraformaldehyde and 1.2 g (0.009 mole) of dibutylamine, and the mixture was reacted, with stirring, at 150° C. for 3 hours. However, the desired product 2,5,7,8-tetramethyl-6-acetoxy-2-hydroxy-methylchroman could not be obtained at all.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05495026 |
|---|
| Source dataset | uspto-grants-1996_02 |
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| ORD ID | ord-c2370559f9a64d2199023b225cc0ecc1 |
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| Source note | uspto-grants-1996_02 |
|---|
