Acetic Acid → HCID 18986671, compound

HRID 2396933Notes

Reaction equation

HRID 2396933 reaction equation
[C:1]([O:4][C:5]1[C:10]([CH3:11])=[CH:9][C:8]([OH:12])=[C:7]([CH3:13])[C:6]=1[CH3:14])(=[O:3])[CH3:2].[C:15]([O:20][CH2:21][CH3:22])(=[O:19])[C:16]([CH3:18])=[CH2:17].C=O.[CH2:25](NCCCC)CCC.C(O)(=O)C>>[CH3:17][C:16]1([C:15]([O:20][CH2:21][CH3:22])=[O:19])[CH2:18][CH2:25][C:9]2[C:8](=[C:7]([CH3:13])[C:6]([CH3:14])=[C:5]([O:4][C:1](=[O:3])[CH3:2])[C:10]=2[CH3:11])[O:12]1

Participants

6

Reactant 5

HCID 176Acetic AcidHCID 712FormaldehydeHCID 7343Ethyl MethacrylateHCID 8148DibutylamineHCID 1190244-Hydroxy-2,3,6-trimethylphenyl acetate

Product 1

HCID 18986671HCID 18986671, compound

Procedure

There were mixed 1.9 g (0.01 mole) of 4-acetoxy-2,3,5-trimethylphenol, 9.2 g (0.08 mole) of ethyl methacrylate, 0.3 g (0.011 mole) of paraformaldehyde, 0.13 g (0.001 mole) of dibutylamine and 0.3 g (0.005 mole) of acetic acid, and the mixture was heated under reflux for 15 hours.

Workup

  1. temperaturethe mixture was heated
  2. temperatureunder reflux for 15 hours

Sources & evidence

ORD record
ord-abad309a89e34eeab8f7d487cec4eada
Source dataset
uspto-grants-1996_02
Patent number
US05495026

Reaction notes

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