Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Dibutylamine | HCID 8148 | — |
| Reactant | 4-Hydroxy-2,3,6-trimethylphenyl acetate | HCID 119024 | — |
| Reactant | 2,6,10,14-tetramethylpentadecene | HCID 11023721 | — |
| Product | Alpha-Tocopherol Acetate | HCID 86472 | — |
Reaction Steps
A pressure-proof reaction vessel equipped with a stirrer was charged with 7.0 g (0.036 mole) of 4-acetoxy-2,3,5-trimethylphenol, 50.0 g (0.18 mole) of 2,6,10,14-tetramethyl-1-pentadecene, 1.4 g (0.045 mole) of 80% paraformaldehyde, 0.5 g (0.0036 mole) of dibutylamine and 1.1 g (0.018 mole) of acetic acid, and the mixture was reacted, with stirring, at 170° C. for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05495026 |
|---|
| Source dataset | uspto-grants-1996_02 |
|---|
| ORD ID | ord-fe89401249404f6e9baed3e54bacbe04 |
|---|
| Source note | uspto-grants-1996_02 |
|---|
