HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 20324732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 20371823 | HCID 20371823 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20324732 | HCID 20324732 | — |
Reaction Steps
A solution was formed containing 25 ml. of benzene and 6 g. of 2-ethyl-5-methyl oxazolidine suspended in 24 ml. of benzene. Then, 5.5 g. of triethylamine was added. The solution was cooled in an ice bath, wherein 5.8 g. of methane sulfonyl chloride was added dropwise with stirring to yield 6.4 g. of product, nD30 = 1.4778.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021229 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-47e8be3b5486498b8867149655b54d37 |
| Source note | uspto-grants-1977_05 |