HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → HCID 12370783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 12370782 | HCID 12370782 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12370783 | HCID 12370783 | — |
Reaction Steps
A mixture of 6-bromomethyl-2-phenylbenzoxazole (40 gm) and sodium cyanide (7.4 gm) in dry dimethylformamide (800 ml) was heated on a steam bath for 3 hr. The mixture was filtered and the filtrate was evaporated to dryness. The solid was recrystallised to give 2-phenyl-6-benzoxazolylacetonitrile as white crystals, m.p. 144° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021440 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-79bed146637f47fa8636aab90887367e |
| Source note | uspto-grants-1977_05 |