N-Methylisatoic anhydride → HCID 21437835, compound

Participants

Reaction Conditions

Reaction Steps

To 65 g. of 1-octanol heated at 108° C. there was added 53.1 g. of N-methylisatoic anhydride in portions during 3.5 hours and the reaction mixture was further heated at 108° C. for 1.75 hours after addition was completed. The reaction mixture was distilled to remove unreacted octanol and to afford the n-octyl N-methylanthranilate as the liquid distillate fraction, b.p. 160°-168° C. at less than 0.1 mm pressure.

Provenance & Evidence