HRID2397286

反应详情

EQUATION

反应方程式

HRID 2397286 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 1 g. of trans/cis methyl 3,7,11-trimethyldodeca-2,4-dienoate, 60 ml. of methanol, 0.5 g. of sodium hydroxide and 6 ml. of water is stirred at about 30° for about 56 hours. The mixture is then diluted with water, neutralized and extracted with ether. The organic phase is washed with water, dried over sodium sulfate and evaporated to yield trans/cis 3,7,11-trimethyldodeca-2,4-dienoic acid.

WORKUP

后处理

  1. additionA mixture of 1 g
  2. extractionextracted with ether
  3. washThe organic phase is washed with water
  4. dry with materialdried over sodium sulfate
  5. customevaporated