HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12612695, compound → HCID 19349187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12612695 | HCID 12612695 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 19349187 | HCID 19349187 | — |
Reaction Steps
One gram of 5% palladium-on-carbon and 8 g. of 2,5-dimethylhex-4-en-1-al is stirred in 50 ml. of ethanol under excess hydrogen at one atomsphere pressure and at room temperature until the theoretical amount of hydrogen is absorbed (about 24 hours). Then, 2 ml. of dichloromethane is added and the mixture filtered. The filtrate is concentrated under reduced pressure to yield 2,5-dimethylhexan-1-al.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021461 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-36bc0de3ac174b83b76a500430da82c6 |
| Source note | uspto-grants-1977_05 |