HRID2397303
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Ethyl N-(4-ethoxycarbonylphenyl)formimidate (Example Ia) (6.7 g, 0.03 mol) and n-butyl 4-methylaminobenzoate (6.2 g, 0.03 mol) were heated at 190° until 1.7 ml of ethanol had been collected by distillation. The solid mass which resulted upon cooling was recrystallized from hexane to yield the product, mp 83°-85° C. ##STR13##
WORKUP
后处理
- distillationhad been collected by distillation
- customThe solid mass which resulted
- temperatureupon cooling
- customwas recrystallized from hexane
- customto yield the product, mp 83°-85° C.