HRID2397303

反应详情

EQUATION

反应方程式

HRID 2397303 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Ethyl N-(4-ethoxycarbonylphenyl)formimidate (Example Ia) (6.7 g, 0.03 mol) and n-butyl 4-methylaminobenzoate (6.2 g, 0.03 mol) were heated at 190° until 1.7 ml of ethanol had been collected by distillation. The solid mass which resulted upon cooling was recrystallized from hexane to yield the product, mp 83°-85° C. ##STR13##

WORKUP

后处理

  1. distillationhad been collected by distillation
  2. customThe solid mass which resulted
  3. temperatureupon cooling
  4. customwas recrystallized from hexane
  5. customto yield the product, mp 83°-85° C.