HRID2397304

反应详情

EQUATION

反应方程式

HRID 2397304 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of ethyl N-(4-ethoxycarbonylphenyl)formimidate (Example Ia) (4.9 g, 0.022 mol) and 2-methoxy-N-methylaniline (3.2 g, 0.022 mol) were heated at 180° until 1.3 ml of ethanol had been collected by distillation. The resulting yellow oil was flash distilled to yield the desired product, bp≈200° C. (0.05 mm). ##STR14##

WORKUP

后处理

  1. distillationhad been collected by distillation
  2. distillationdistilled