HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 68125000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 2-Buten-1-amine | HCID 30447 | — |
| Reactant | 8-(methylthio)-1-(chloromethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine | HCID 20361160 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68125000 | HCID 68125000 | — |
Reaction Steps
In the manner given in Example 32, 8-(methylthio)-1-(chloromethyl)-6-phenyl-4H-s-triazolo[4,3- a][1,4]benzodiazepine, potassium iodide, and methylallylamine in tetrahydrofuran are reacted to give 8-(methylthio)-1-[(allylmethylamino)methyl]-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021441 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-0c62465578514341b39a477fce06dd85 |
| Source note | uspto-grants-1977_05 |