Cyclohexylamine → HCID 21437992, compound

HRID 2397377Notes

Reaction equation

HRID 2397377 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[CH:14]=[CH:13][C:12]([CH:15](O)[CH2:16][CH2:17][C:18]([OH:20])=[O:19])=[CH:11][CH:10]=1.C1(N)CCCCC1>O>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][CH2:17][C:18]([OH:20])=[O:19])=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 21437946HCID 21437946, compound

Product 1

HCID 21437992HCID 21437992, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Prepared analogous to Example 9 from 4-(2',4'-dichloro-4-biphenylyl)-4-hydroxy-butyric acid. Melting point of the cyclohexylamine salt: 154°-155° C. (from water).

Sources & evidence

ORD record
ord-9f96ebe1b3b54da2b4e3f6d028e87e36
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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