Cyclohexylamine → HCID 15541122, compound

HRID 2397393Notes

Reaction equation

HRID 2397393 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([C:14](=[O:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.C1(N)CCCCC1>O>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[CH:13]=[CH:12][C:11]([CH:14]([OH:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 14116665HCID 14116665, compound

Product 1

HCID 15541122HCID 15541122, compoundYield 61%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Prepared analogous to Example 25 from 4-(4'-chloro-4-biphenylyl)-4-oxo-butyric acid. Melting point of the cyclohexylamine salt: 185°-186° C. (from water). Yield: 61% of theory.

Sources & evidence

ORD record
ord-ecfac8dc69774b789507318d45e77452
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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