Cyclohexylamine → HCID 21437908, compound

HRID 2397394Notes

Reaction equation

HRID 2397394 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][C:11]([C:14](=[O:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.C1(N)CCCCC1>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[CH:13]=[CH:12][C:11]([CH:14]([OH:20])[CH2:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 7965CyclohexylamineHCID 14116663HCID 14116663, compound

Product 1

HCID 21437908HCID 21437908, compoundYield 70%

Procedure

Prepared analogous to Example 25 from 4-(4'-bromo-4-biphenylyl)-4-oxo-butyric acid. Yield: 70% of theory; m.p. 127° C. Melting point of the cyclohexylamine salt: 193° C.

Workup

  1. custom193° C.

Sources & evidence

ORD record
ord-b804e623c4a943858edbbedeec8df0cb
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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