Cyclohexylamine → HCID 21437916, compound

HRID 2397398Notes

Reaction equation

HRID 2397398 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[CH:15]=[CH:14][C:13]([C:16](=[O:22])[CH2:17][CH2:18][C:19]([OH:21])=[O:20])=[CH:12][CH:11]=1)([O-:3])=[O:2].C1(N)CCCCC1>>[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10]1[CH:15]=[CH:14][C:13]([CH:16]([OH:22])[CH2:17][CH2:18][C:19]([OH:21])=[O:20])=[CH:12][CH:11]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 7965CyclohexylamineHCID 21437958HCID 21437958, compound

Product 1

HCID 21437916HCID 21437916, compoundYield 62.5%

Procedure

Prepared analogous to Example 25 from 4-(2'-nitro-4-biphenylyl)-4-oxo-butyric acid. Yield: 62.5% of theory; m.p. 114°-115° C.; melting point of the cyclohexylamine salt; 170° C. (decomp.).

Sources & evidence

ORD record
ord-94d4e9cb6a29448285dc35c08cc4f50a
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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