Cyclohexylamine → HCID 21437965, compound

HRID 2397399Notes

Reaction equation

[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:15]=[CH:14][C:13]([C:16](=[O:22])[CH2:17][CH2:18][C:19]([OH:21])=[O:20])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].C1(N)CCCCC1>>[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([C:10]2[CH:15]=[CH:14][C:13]([CH:16]([OH:22])[CH2:17][CH2:18][C:19]([OH:21])=[O:20])=[CH:12][CH:11]=2)=[CH:8][CH:9]=1)([O-:3])=[O:2]

Participants

Reactant 2

HCID 7965Cyclohexylamine

HCID 21437944HCID 21437944, compound

Product 1

HCID 21437965HCID 21437965, compoundYield 45%

Procedure

Prepared analogous to Example 25 from 4-(4'-nitro-4-biphenylyl)-4-oxo-butyric acid. Yield: 45% of theory; m.p. 153° C. (decomp.); melting point of the cyclohexylamine salt: 178°-179° C. (decomp.).

Sources & evidence

ORD record: ord-061feb7e1f564142839db337650fc779
Source dataset: uspto-grants-1977_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04021479

Reaction notes

Loading…