Cyclohexylamine → HCID 21437946, compound

HRID 2397406Notes

Reaction equation

HRID 2397406 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[CH:14]=[CH:13][C:12]([C:15](=[O:21])[CH2:16][CH2:17][C:18]([OH:20])=[O:19])=[CH:11][CH:10]=1.C1(N)CCCCC1>O>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[CH:14]=[CH:13][C:12]([CH:15]([OH:21])[CH2:16][CH2:17][C:18]([OH:20])=[O:19])=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 21437974HCID 21437974, compound

Product 1

HCID 21437946HCID 21437946, compoundYield 70%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Prepared analogous to Example 42 from 4-(2',4'-dichloro-4-biphenylyl)-4-oxo-butyric acid. Yield: 70% of theory. Melting point of the cyclohexylamine salt: 168°-169° C. (from water).

Sources & evidence

ORD record
ord-16dda57045d3451c9f3a8f72e4307cf3
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

Loading…