Cyclohexylamine → HCID 21437924, compound

HRID 2397409Notes

Reaction equation

HRID 2397409 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([C:8](=[O:14])[CH2:9][CH2:10][C:11]([OH:13])=[O:12])[CH:5]=[CH:4][C:3]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.C1CCCCC1.CCOCC.C1(N)CCCCC1>CC(C)=O.C(OCC)(=O)C>[Cl:1][C:2]1[CH:7]=[C:6]([CH:8]([OH:14])[CH2:9][CH2:10][C:11]([OH:13])=[O:12])[CH:5]=[CH:4][C:3]=1[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

Participants

5

Reactant 3

HCID 7965CyclohexylamineHCID 21437923HCID 21437923, compoundHCID 21895417Cyclohexane diethylether

Product 1

HCID 21437924HCID 21437924, compound

Reagents, catalysts & solvents 1

HCID 21584569Ethylacetate acetoneSolvent

Procedure

Prepared analogous to Example 42 from 4-(2-chloro-4-biphenylyl)-4-oxo-butyric acid. Melting point 87°-88° C. (from cyclohexane/ether); melting point of the cyclohexylamine salt: 156°-157° C. (from acetone/ethyl acetate).

Sources & evidence

ORD record
ord-7cfaa6db1ab04c98bb1aa5a587352f06
Source dataset
uspto-grants-1977_05
Patent number
US04021479

Reaction notes

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