HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 21313327, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21313303 | HCID 21313303 | — |
| Reactant | HCID 21313349 | HCID 21313349 | — |
| Reactant | HCID 21313368 | HCID 21313368 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21313327 | HCID 21313327 | — |
Reaction Steps
1-Benzoyl-3-[2-(2-cyclohexylmethylpiperidino)ethyl]-5-t-butoxy-2-methylindole is prepared by reaction of 4-t-butoxyphenylhydrazine with 1-(2-cyclohexylmethylpiperidino)pentan-4-one in ethanol and reaction of the resulting 3-[2-(2-cyclohexylmethylpiperidino)ethyl]-5-t-butoxy-2-methylindole with sodium hydride in DMF followed by reaction of the resulting sodium salt with benzoyl chloride all according to the procedure described above in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04021431 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-a4ed5eda1e3b4c239a2c565d6841525d |
| Source note | uspto-grants-1977_05 |