HCID 21436325, compound → HCID 21436339, compound

HRID 2397626Notes

Reaction equation

HRID 2397626 reaction equation
[OH:1]C(CCCCC)CCN1C(=O)CS(=O)C1CCCCCCC(O)=O.[OH:26][CH:27]([CH2:46][O:47][CH2:48][CH2:49][CH3:50])[CH2:28][CH2:29][N:30]1[C:34](=[O:35])[CH2:33][S:32](=[O:36])[CH:31]1[CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][C:43]([OH:45])=[O:44]>>[OH:26][CH:27]([CH2:46][O:47][CH2:48][CH2:49][CH3:50])[CH2:28][CH2:29][N:30]1[C:34](=[O:35])[CH2:33][S:32](=[O:1])(=[O:36])[CH:31]1[CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][C:43]([OH:45])=[O:44]

Participants

3

Reactant 2

HCID 21436325HCID 21436325, compoundHCID 21436340HCID 21436340, compound

Product 1

HCID 21436339HCID 21436339, compound

Procedure

This compound is prepared essentially by the same procedure as described in Example 3 except that the 7-[3-(3-hydroxyoctyl)-1,4-dioxo-2-thiazolidinyl]heptanoic acid is replaced by 7-[3-(3-hydroxy-4-propoxybutyl)-1,4-dioxo-2-thiazolidinyl]heptanoic acid. Chromatographic purification of the resulting product on silica gel gives the title compound as a viscous, pale yellow oil.

Workup

  1. customThis compound is prepared essentially by the same procedure
  2. customChromatographic purification of the resulting product on silica gel

Sources & evidence

ORD record
ord-45287e3e0b274d85a90103f9493312fa
Source dataset
uspto-grants-1977_05
Patent number
US04022794

Reaction notes

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