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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2397674Generated: October 25, 2026

2-Benzylidenebutanoic acid → 2-Benzylbutanoic acid

https://huagongshe.com/reaction/2397674

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Benzylidenebutanoic acidHCID 235117—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventSodium HydroxideHCID 14798—
Product2-Benzylbutanoic acidHCID 21881100%

Reaction Steps

A solution of 35.2 gm (0.2 mol) of α-ethyl cinnamic acid in 450 ml of 3% sodium hydroxide was reduced in a hydrogen atmosphere at 60 psi using 4 gm of 5% palladium on charcoal. After hydrogen uptake had ceased, the reaction mixture was filtered, acidified with hydrochloric acid and extracted with ether. Evaporation gave 36 gm (0.2 mol) of 2-benzyl butanoic acid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04022814
Source datasetuspto-grants-1977_05
ORD IDord-bae2a6957965486d905a0c1e072beae2
Source noteuspto-grants-1977_05