HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 21436542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2,3,4,5-Tetrachloro-6-hydroxybenzonitrile | HCID 21436544 | — |
| Product | HCID 21436542 | HCID 21436542 | 97% |
Reaction Steps
a 10.0 g portion of this hydroxy-tetrachlorobenzonitrile was heated under an inert atmosphere at 130° C. for 15 minutes with 150 ml concentrated sulfuric acid. The product, hydroxytetrachlorobenzamide was readily isolated by filtering the H2O-diluted reaction mixture; yield 97.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022830 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-001ccdc0c316481fa977c178a5317aa8 |
| Source note | uspto-grants-1977_05 |