HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenediamine → N,N'-(1,6-hexylene)-bis[2-hydroxynonylamine]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | 2-Heptyloxirane | HCID 551181 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N,N'-(1,6-hexylene)-bis[2-hydroxynonylamine] | HCID 21332345 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-nonene oxide (97.4 g.) and hexamethylenediamine (39.8 g.) and recrystallization of the resulting product (67g.) from ethanol afforded N,N'-(1,6-hexylene)-bis[2-hydroxynonylamine] (I: R= CH3 (CH2)6, R' = H, X= (CH2)6, Z= H) (67 g., m.p. 122°-129.2° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022833 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-8f40bfeff71c48598d9873de14ee3f4d |
| Source note | uspto-grants-1977_05 |