Hexamethylenediamine → HCID 21332371, compound

HRID 2397803Notes

Reaction equation

HRID 2397803 reaction equation
[CH2:1]1[O:11][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[NH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][NH2:19]>CO>[CH2:18]([NH:19][CH2:1][CH:2]([OH:11])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][NH:12][CH2:1][CH:2]([OH:11])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 16402HexamethylenediamineHCID 169931,2-Epoxydecane

Product 1

HCID 21332371HCID 21332371, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a manner similar to that of Example 1, condensation of 1-decene oxide (50 g.) and hexamethylenediamine (18.6 g.) and recrystallization of the resulting product from methanol gave N,N'-(1,6-hexylene)-bis[2-hydroxydecylamine] (I: R= CH3 (CH2)7, R' = H, X= (CH2)6, Z= H) (25.4 g., m.p. 118.0°-126.8° C.).

Sources & evidence

ORD record
ord-c40af8fed69543b794aae3d8e6042b24
Source dataset
uspto-grants-1977_05
Patent number
US04022833

Reaction notes

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