HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenediamine → HCID 21332441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | 1,2-Epoxydodecane | HCID 17858 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21332441 | HCID 21332441 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-dodecene oxide (50 g.) and hexamethylenediamine (15.8 g.) and recrystallization of the resulting product from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxydodecylamine] (I: R= CH3 (CH2)9, R' = H, X= (CH2)6, Z= H) (35 g., m.p. 123.6°-128.0° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022833 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-d3c60d5724884872b47cff65bb87f02d |
| Source note | uspto-grants-1977_05 |