HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenediamine → N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | 1,2-Epoxytetradecane | HCID 18604 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] | HCID 21332395 | — |
Reaction Steps
In a manner similar to that of Example 1, condensation of 1-tetradecene oxide (91.8 g.) and hexamethylenediamine (25 g.) and recrystallization of the resulting product (71 g., m.p. 118°-121° C.) from ethanol gave N,N'-(1,6-hexylene)-bis[2-hydroxytetradecylamine] (I: R= CH3 (CH2)11, R' = H, X== (CH2)6, Z= H) (55.3 g., m.p. 122°-126° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022833 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-88527bd7667c46238f5b586c7d5b0307 |
| Source note | uspto-grants-1977_05 |