1,3-Propanediamine → HCID 21332393, compound

HRID 2397820Notes

Reaction equation

HRID 2397820 reaction equation
[CH2:1]1[O:11][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH2:12]([NH2:16])[CH2:13][CH2:14][NH2:15]>CO>[CH2:12]([NH:16][CH2:1][CH:2]([OH:11])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:13][CH2:14][NH:15][CH2:1][CH:2]([OH:11])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 4281,3-PropanediamineHCID 169931,2-Epoxydecane

Product 1

HCID 21332393HCID 21332393, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a manner similar to that of Example 1, condensation of 1-decene oxide (58 g.) and 1,3-propanediamine (13.8 g.) and three recrystallizations of the resulting product from methanol gave N,N'-(1,3-propylene)-bis[2-hydroxydecylamine] (I: R= CH3 (CH2)7, R' = H, X= (CH2)3, Z= H) (8.5 g., m.p. 104.0°-107.6° C.).

Sources & evidence

ORD record
ord-9a35a761a4194085a18920a1e163999b
Source dataset
uspto-grants-1977_05
Patent number
US04022833

Reaction notes

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