化工社化工社 化学情報印刷レポート · 研究参考用
1,10-Decanediamine → N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine]
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,10-Decanediamine | HCID 1317 | — |
| 反応物 | 2-Butyloxirane | HCID 15036 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine] | HCID 21332454 | 13.7% |
反応手順
In a manner similar to that of Example 1, condensation of 1-hexene oxide (34.8 g.) and 1,10-decanediamine (30 g.) and recrystallization of the resulting product from isopropyl alcohol gave N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine] (I: R= CH3 (CH2)3R' = H, X= (CH2)10, Z= H) (8.9 g., m.p. 127.0°-137.0° C.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04022833 |
| 出典データセット | uspto-grants-1977_05 |
| ORD ID | ord-6ba143f1a9f345d0aa0fb5f9c7336909 |
| 出典メモ | uspto-grants-1977_05 |