HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminoisoquinoline → HCID 8763133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminoisoquinoline | HCID 70766 | — |
| Reactant | Benzoyl chloride, 3,4,5-trimethoxy- | HCID 78282 | — |
| Product | HCID 8763133 | HCID 8763133 | — |
Reaction Steps
3,4,5-Trimethoxybenzoyl chloride was reacted with 5-aminoisoquinoline according to the procedure of Example 8 to produce 5-(3,4,5-trimethoxybenzamido) isoquinoline. This product was then reduced according to the procedure of Example 8 to yield 5-(3,4,5-trimethoxybenzamido)-1,2,3,4-tetrahydroisoquinoline HCl. After purification from methanol it had a melting point of 270°-271.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022900 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-ceaeed1afac8419b8ff5295b26722ad2 |
| Source note | uspto-grants-1977_05 |