Benzoyl chloride → HCID 86734726, compound

HRID 2397951Notes

Reaction equation

HRID 2397951 reaction equation
[OH:1][C@@H:2]1[C@@:27]2([CH3:28])[C:6](=[CH:7][CH2:8][C@@H:9]3[C@@H:26]2[CH2:25][CH2:24][C@@:23]2([CH3:29])[C@H:10]3[CH2:11][CH2:12][C@@H:13]2[C@H:14]([CH3:22])[CH2:15][CH2:16][CH:17]([OH:21])[CH:18]([CH3:20])[CH3:19])[CH2:5][C@@H:4]([OH:30])[CH2:3]1.[C:31](Cl)(=[O:38])[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1>N1C=CC=CC=1>[C:2]([OH:1])(=[O:38])[C:27]1[CH:6]=[CH:7][CH:8]=[CH:9][CH:26]=1.[C:31]([OH:38])(=[O:1])[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1.[OH:1][C@@H:2]1[C@@:27]2([CH3:28])[C:6](=[CH:7][CH2:8][C@@H:9]3[C@@H:26]2[CH2:25][CH2:24][C@@:23]2([CH3:29])[C@H:10]3[CH2:11][CH2:12][C@@H:13]2[C@H:14]([CH3:22])[CH2:15][CH2:16][CH:17]([OH:21])[CH:18]([CH3:20])[CH3:19])[CH2:5][C@@H:4]([OH:30])[CH2:3]1

Participants

4

Reactant 2

HCID 7412Benzoyl chlorideHCID 10938669HCID 10938669, compound

Product 1

HCID 86734726HCID 86734726, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

2.5 g of 1α,24-dihydroxycholesterol was mixed with 2.10 g of benzoyl chloride and 40 ml. of pyridine, and the mixture was allowed to stand for one day at 20° C.

Sources & evidence

ORD record
ord-e998265dc48d49048803338f8537b375
Source dataset
uspto-grants-1977_05
Patent number
US04022891

Reaction notes

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