HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 60965-80-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 70634974 | HCID 70634974 | — |
| Product | 60965-80-2 | HCID 6437387 | — |
| Product | HCID 53837977 | HCID 53837977 | — |
Reaction Steps
20 mg of 1α-hydroxy-3β,24-dibenzoyloxycholesta-5,7-diene was dissolved in 500 ml. of diethyl ether. The solution was irradiated with ultraviolet rays, isomerized, and hydrolyzed in the same way as in Example 21, (B) to afford 1.9 mg of 1α,24-dihydroxycholecalciferol which showed the same properties as the product obtained in Example 20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04022891 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-f8af7baee9d94c6991dd40ff60ccff60 |
| Source note | uspto-grants-1977_05 |