HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21395237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 4-bromobutyrate | HCID 107604 | — |
| Reactant | N-4-Piperidylbenzamide | HCID 118120 | — |
| Product | HCID 21395237 | HCID 21395237 | 82% |
Reaction Steps
An intimate mixture of 4-benzamidopiperidine (2.0g.), methyl 4-bromobutyrate (2.0g.) and potassium carbonate (1.5 g.) was stirred and heated on a steam bath for 15 minutes. An exothermic reaction occured and the semi-molten mixture set solid. Trituration with water (20 ml.) and filtration provided the title compound (2.41 g., 82%), m.p. 116°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024147 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-6c464d417ff84b4ca1f902dcaa268f49 |
| Source note | uspto-grants-1977_05 |