Cycloheptylamine → HCID 21434456, compound

HRID 2398179Notes

Reaction equation

C(O[C:4](=[O:25])[NH:5][S:6]([C:9]1[CH:24]=[CH:23][C:12]2[CH2:13][CH2:14][N:15]([C:18](=[O:22])[N:19]([CH3:21])[CH3:20])[CH2:16][CH2:17][C:11]=2[CH:10]=1)(=[O:8])=[O:7])C.[CH:26]1([NH2:33])[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27]1>>[CH:26]1([NH:33][C:4]([NH:5][S:6]([C:9]2[CH:24]=[CH:23][C:12]3[CH2:13][CH2:14][N:15]([C:18](=[O:22])[N:19]([CH3:20])[CH3:21])[CH2:16][CH2:17][C:11]=3[CH:10]=2)(=[O:8])=[O:7])=[O:25])[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27]1

Participants

Reactant 2

HCID 2899Cycloheptylamine

HCID 53895465HCID 53895465, compound

Product 1

HCID 21434456HCID 21434456, compound

Procedure

By the reaction of [(3-dimethylcarbamoyl-2,3,4,5-tetrahydro-1-H-3-benzazepin-7-yl)sulfonyl]carbamic acid ethyl ester with cycloheptylamine in a manner analogous to that described in Example 12, there is obtained 1-cycloheptyl-3-[(3-dimethylcarbamoyl-2,3,4,5-tetrahydro-1H-3-benzazepin-7-yl)sulfonyl]urea.

Sources & evidence

ORD record: ord-7e7a5dc5cafb4726b468532533f858f5
Source dataset: uspto-grants-1977_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04024128

Reaction notes

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