HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Bis(methylthio)-2-nitroethylene → HCID 70546477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | HCID 12923401 | HCID 12923401 | — |
| Product | HCID 70546477 | HCID 70546477 | — |
Reaction Steps
By the procedure of Example 4(i), 2-(3-aminopropylthio)-imidazole (from the dihydrobromide (3.8 g)) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) to give 1-nitro-2-methylthio-2-[3-(2-imidazolylthio)propylamino]ethylene which, on treatment with methylamine according to the procedure of Example 3(ii) gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024260 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-7bfea42c70364f4283b7737831b5d674 |
| Source note | uspto-grants-1977_05 |