HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178484399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | HCID 178503827 | HCID 178503827 | — |
| Reactant | HCID 178511474 | HCID 178511474 | — |
| Product | HCID 178484399 | HCID 178484399 | — |
Reaction Steps
4-[2-(2-Aminoethylthio)ethyl]imidazole (from the dihydrobromide (4.0 g)) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) by the procedure of Example 4(i) and the resultant 1-nitro-2-methylthio-2-[2-(2-(4-imidazolyl)ethylthio)ethylamino]-ethylene is treated with methylamine according to the procedure of Example 3(ii) to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024260 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-e0f06edf506d4d96a4be16c05361b1dc |
| Source note | uspto-grants-1977_05 |