HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 70542314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| Reactant | 2-((Isoxazol-3-ylmethyl)thio)ethanamine | HCID 12923417 | — |
| Reactant | 1-Nitro-2-methylthio-2-[2-(3-isoxazolylmethylthio)ethylamino]ethylene | HCID 70544411 | — |
| Product | HCID 70542314 | HCID 70542314 | — |
Reaction Steps
Reaction of 3-[(2-aminoethyl)thiomethyl]isoxazole (from the dihydrobromide (3.8 g) with 1-nitro-2,2-bis-methylthioethylene (2.0 g) by the procedure of Example 4(i) and treatment of the resultant 1-nitro-2-methylthio-2-[2-(3-isoxazolylmethylthio)ethylamino]ethylene with methylamine according to the procedure of Example 3(ii) gives 1-nitro-2-methylamino-2-[2-(3-isoxazolylmethylthio)ethylamino]-ethylene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024260 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-ab501e6b3c7142d3ac39cb6364b115dd |
| Source note | uspto-grants-1977_05 |