Thionyl Chloride → HCID 12366428, compound

HRID 2398273Notes

Reaction equation

HRID 2398273 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=[O:7])=[C:4]([O:11][C:12](=[O:14])[CH3:13])[CH:3]=1.S(Cl)([Cl:17])=O>>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([Cl:17])=[O:7])=[C:4]([O:11][C:12](=[O:14])[CH3:13])[CH:3]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 1527825814504-07-5

Product 1

HCID 12366428HCID 12366428, compound

Procedure

4-Methyl-2-acetoxy-benzoic acid (18 g.) was dissolved in thionyl chloride (200 ml.), and the solution was left to stand overnight at room temperature. Removal of excess thionyl chloride by suction gave a paste of crude 4-methyl-2-acetoxy-benzoyl chloride which was dissolved in acetone (200 ml.).

Workup

  1. waitthe solution was left
  2. customRemoval of excess thionyl chloride by suction

Sources & evidence

ORD record
ord-dadde669f14d4cdb83f51866acc240c0
Source dataset
uspto-grants-1977_05
Patent number
US04024253

Reaction notes

Loading…