HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 6-Thiatetracycline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178482997 | HCID 178482997 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 6-Thiatetracycline | HCID 54676882 | — |
Reaction Steps
467 mg of 7-chloro-6-thiatetracycline in 25 ml of methanol are hydrogenated in the presence of 101 mg of triethylamine on 200 mg of 10% Pd-on-charcoal at 20° and normal pressure to give 6-thiatetracycline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04024272 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-f3ec6552c23244cb9e6e699c65b2e1da |
| Source note | uspto-grants-1977_05 |