HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 22261712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Mono-Methyl Succinate | HCID 6930703 | — |
| Product | HCID 22261712 | HCID 22261712 | — |
Reaction Steps
Methyl succinate (20.5 g) was heated with 20 ml thionyl chloride to 40° for 3.5 hours. Excess thionyl chloride was removed by vacuum distillation (13 mm Hg). The acid chloride (20.6 g) was distilled at 43°-44° /0.2 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025501 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-4d56c713f26c44d0b57b7c4974509ca4 |
| Source note | uspto-grants-1977_05 |