HCID 68119223, compound → HCID 68119722, compound

Participants

Reaction Steps

The mixture of 10.0 g of N-(4-nitro-o-tolyl)-4-fluorophthalimide, 500 ml of ethyl acetate and 5 g of Raney nickel is hydrogenated at 3.1 atm. and room temperature until the hydrogen uptake ceases. It is filtered, evaporated, and the residue recrystallized from ethanol, to yield the N-(4-amino-o-tolyl)-4-fluorophthalimide, melting at 180°-182°.

Provenance & Evidence