HCID 68120111, compound → HCID 68118656, compound

Participants

Reaction Steps

The mixture of 6.5 g of N-(4-nitro-o-tolyl)-4-dimethylcarbamoylphthalimide, 3.0 g of Raney nickel and 270 ml of ethyl acetate is hydrogenated at 3.1 atm. and room temperature until the hydrogen uptake ceases. It is filtered, the filtrate evaporated, the residue washed with hot ethanol and dried, to yield the N-(4-amino-o-tolyl)-4-dimethylcarbamoylphthalimide melting at 214°-217°.

Provenance & Evidence