HCID 131710789, compound → HCID 131710788, compound

Participants

Reaction Steps

The mixture of 1.7 g of N-(4-nitro-o-tolyl)-5-chlorohomophthalimide, 0.8 g of Raney nickel and 250 ml of ethyl acetate is hydrogenated at 2.4 atm. and room temperature until the hydrogen uptake has ceased. It is filtered, the filtrate evaporated and the residue recrystallized from acetonitrile to yield the N-(4-amino-o-tolyl)-5-chlorohomophthalimide of the formula ##STR7## melting at 250°-252° with decomposition.

Provenance & Evidence