HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68119419, compound → HCID 68118990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68119419 | HCID 68119419 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68118990 | HCID 68118990 | — |
Reaction Steps
The solution of 1.0 g of N-(4-nitro-o-tolyl)-4-methoxyphthalimide in 70 ml of ethyl acetate is hydrogenated over 0.35 g of platinum oxide at 2.5 atm. and room temperature for 2 hours. It is filtered, the filtrate concentrated and the precipitate formed collected, to yield the N-(4-amino-o-tolyl)-4-methoxyphthalimide melting at 158°-161°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04025505 |
| Source dataset | uspto-grants-1977_05 |
| ORD ID | ord-c45025fd250d4d9299bcf170764f5311 |
| Source note | uspto-grants-1977_05 |