HCID 131710791, compound → HCID 131710790, compound

Participants

Reaction Steps

The solution of 0.5 g of N-(4-nitro-o-tolyl)-4-chloro-α-methylhomophthalimide in 120 ml of ethyl acetate is hydrogenated over 2.0 g of Raney nickel (washed with water and ethanol) at 2.5 atm. and room temperature for 5 hours. It is filtered and the filtrate evaporated, to yield the N-(4-amino-o-tolyl)-4-chloro-α-methylhomophthalimide of the formula ##STR8## showing in the I.R.-spectrum bands at 1665 and 1710cm-1 and in the mass-spectrum the ion of 314/316.

Provenance & Evidence